Synthesis of 10,11,14,15‐ 13 C 4 ‐and 14,15‐ 13 C 2 ‐retinyl acetate | Zendy

Tanumihardjo Sherry A. | Zendy

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Synthesis of 10,11,14,15‐ 13 C 4 ‐and 14,15‐ 13 C 2 ‐retinyl acetate

Author(s) -

Tanumihardjo Sherry A.

Publication year - 2001

Publication title -

journal of labelled compounds and radiopharmaceuticals

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.432

H-Index - 47

eISSN - 1099-1344

pISSN - 0362-4803

DOI - 10.1002/jlcr.464

Subject(s) - chemistry , isotope dilution , retinyl acetate , isotope , mass spectrometry , chromatography , specific activity , radiochemistry , organic chemistry , biochemistry , retinol , vitamin , enzyme , physics , quantum mechanics

The synthesis of 10,11,14,15‐ 13 C 4 ‐ and 14,15‐ 13 C 2 ‐retinyl acetate is described. The procedure uses a modified Wittig‐Horner synthesis. By using the 13 C isotope, sensitive gas chromatography‐combustion‐isotope ratio mass spectrometry can be used for analysis in application to human isotope dilution studies. Copyright © 2001 John Wiley & Sons, Ltd.

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