Synthesis of stable isotope labeled D 9 ‐Mabuterol, D 9 ‐Bambuterol, and D 9 ‐Cimbuterol | Zendy

Tu Yahui | Zendy; Zhong Jiaqi | Zendy; Wang Haoran | Zendy; Pan Jie | Zendy; Xu Zhongjie | Zendy; Yang Weicheng | Zendy; Luo Yong | Zendy

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Synthesis of stable isotope labeled D 9 ‐Mabuterol, D 9 ‐Bambuterol, and D 9 ‐Cimbuterol

Author(s) -

Tu Yahui,

Zhong Jiaqi,

Wang Haoran,

Pan Jie,

Xu Zhongjie,

Yang Weicheng,

Luo Yong

Publication year - 2016

Publication title -

journal of labelled compounds and radiopharmaceuticals

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.432

H-Index - 47

eISSN - 1099-1344

pISSN - 0362-4803

DOI - 10.1002/jlcr.3446

Subject(s) - chemistry , isotope , natural abundance , stable isotope ratio , abundance (ecology) , mass spectrometry , chromatography , radiochemistry , tandem , nuclear physics , physics , biology , materials science , fishery , composite material

Three stable and simple synthetic routes of labeled D 9 ‐Mabuterol, D 9 ‐Bambuterol, and D 9 ‐Cimbuterol were described with 98.5%, 99.7%, and 98.4% isotopic abundance and good purity. These structures and isotope‐abundance were confirmed according to 1 H NMR and liquid chromatography‐tandem mass spectrometry.

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