Synthesis of isotopically labelled 2‐isopropylthioxanthone from 2,2′‐dithiosalicylic acid and deuterium cumene | Zendy

Fang Chao | Zendy; Yang Weicheng | Zendy; Yang Chao | Zendy; Wang Haoran | Zendy; Sun Kai | Zendy; Luo Yong | Zendy

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Synthesis of isotopically labelled 2‐isopropylthioxanthone from 2,2′‐dithiosalicylic acid and deuterium cumene

Author(s) -

Fang Chao,

Yang Weicheng,

Yang Chao,

Wang Haoran,

Sun Kai,

Luo Yong

Publication year - 2016

Publication title -

journal of labelled compounds and radiopharmaceuticals

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.432

H-Index - 47

eISSN - 1099-1344

pISSN - 0362-4803

DOI - 10.1002/jlcr.3400

Subject(s) - chemistry , deuterium , natural abundance , mass spectrometry , cumene , abundance (ecology) , radiochemistry , isotope , tritium , carbon 13 , proton , chromatography , organic chemistry , nuclear physics , benzene , physics , fishery , biology

Two efficient synthetic routes of stable deuterium labelled 2‐isopropylthioxanthone were presented with 98.1% and 98.8% isotopic abundance in acceptable yields and excellent chemical purities. Their structures and the isotope‐abundance were confirmed according to proton nuclear magnetic resonance and liquid chromatography–mass spectrometry.

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