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A convenient preparation of 18 O‐dimethylformamide
Author(s) -
Rao Koganty R.,
Digenis George A.
Publication year - 1974
Publication title -
journal of labelled compounds
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0022-2135
DOI - 10.1002/jlcr.2590100308
Subject(s) - dimethylformamide , chloride , chemistry , benzoyl chloride , nuclear chemistry , organic chemistry , solvent
A method is described by which 18 O‐DMF can be prepared conveniently and in very high yields (∼ 90%) by reacting at room temperature an equimolar quantity of benzoyl chloride, DMF and 18 O‐labelled water.