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Synthesis of carbon‐14 labelled S‐ethyl hexahydro‐1H‐azepine‐1‐carbothiolate
Author(s) -
Gutman A. D.,
Baker D. R.,
Brokke M. E.
Publication year - 1966
Publication title -
journal of labelled compounds
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0022-2135
DOI - 10.1002/jlcr.2590020211
Subject(s) - azepine , moiety , yield (engineering) , residue (chemistry) , chemistry , carbon 14 , ring (chemistry) , organic chemistry , nuclear chemistry , materials science , physics , quantum mechanics , metallurgy
S‐Ethyl hexahydro‐1H‐azepine‐1‐carbothiolate labelled in the ethyl moiety and in the azepine ring with carbon‐14 was prepared to facilitate residue and metabolism studies. The ethyl labeled compound was prepared in 86% yield and 99+% radiochemical purity. The azepine labeled material was prepared in 60% yield and 99+% radiochemical purity.