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Preparation of labelled compounds by tritioboration procedures I. cyclohexene‐1‐ 3 H
Author(s) -
Buczkowski Z.,
Nystrom R. F.
Publication year - 1965
Publication title -
journal of labelled compounds
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0022-2135
DOI - 10.1002/jlcr.2590010405
Subject(s) - cyclohexene , yield (engineering) , chemistry , tritium , valeric acid , carbon atom , carbon fibers , carbon 14 , medicinal chemistry , organic chemistry , radiochemistry , catalysis , acetic acid , mathematics , materials science , ring (chemistry) , nuclear physics , physics , algorithm , composite number , metallurgy
Cyclohexene‐1‐ 3 H has been synthesized with a yield of 88% by tritioboration of 1‐(N‐piperidino)‐cyclohexene followed by heating with n‐valeric acid. Other unsaturated compounds can be labelled at one olefinic carbon atom with tritium by this method.