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Synthesis and spectroscopic characterisation of 3‐chloroperbenzoic acid‐ 17 O, 18 O, nitrosobenzene‐ 17 O, 18 O and nitrosobenzene‐ 15 N
Author(s) -
Bleasdale Christine,
Ellis Martin K.,
Farmer Peter B.,
Golding Bernard T.,
Handley Kevin F.,
Jones Peter,
McFarlane William
Publication year - 1993
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/jlcr.2580330810
Subject(s) - nitrosobenzene , nitrobenzene , chemistry , aniline , hydrogen peroxide , medicinal chemistry , nuclear chemistry , organic chemistry , catalysis
3‐Chloroperbenzoic acid‐ 17 O, 18 O was prepared from 3‐chlorobenzoyl chloride and hydrogen peroxide‐ 17 O, 18 O (obtained by subjecting water‐ 17 O, 18 O. Nitrobenzene‐ 15 N was reduced to aniline‐ 15 N, which was oxidised by 3‐chloroperbenzoic acid to nitrosobenzene‐ 15 N. 15 N and 17 O NMR data are given for the corresponding labelled nitrosobenzene.