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Preparation of 14 C‐ and 18 O‐enriched allyl alcohol (propanol free)
Author(s) -
KupczykSubotkowska Lidai,
Shine Henry J.
Publication year - 1992
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/jlcr.2580310507
Subject(s) - chemistry , allyl alcohol , alcohol , propanol , radiochemistry , medicinal chemistry , nuclear chemistry , organic chemistry , methanol , catalysis
Preparations of specifically labeled [1‐ 14 C]‐, [3‐ 14 C]‐ and [1‐ 18 O]allyl alcohol are described. The syntheses were achieved, respectively, in 7, 11 and 9 steps, with overall yields of 33%, 10% and 38%. Commercially available K 14 CN, CH 3 14 COONa and H 2 18 O were used as the starting materials.