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Synthesis of 3‐methyl‐15‐phenyl‐[carboxyl‐ 14 C]‐pentadecanoic acid
Author(s) -
Humbert T.,
LuuDuc C.,
Le Bars D.,
Vidal M.,
Apparu M.
Publication year - 1988
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/jlcr.2580250919
Subject(s) - chemistry , pentadecanoic acid , yield (engineering) , carbon 14 , medicinal chemistry , radiochemistry , organic chemistry , fatty acid , materials science , physics , quantum mechanics , metallurgy
B‐Methyl‐15‐phenyl‐pentadecanoic acid labelled with carbon‐14 was obtained with good yield in two steps from Na 14 CN, starting from 14‐methyl 1‐phenyl‐ tetradecanol methanesulfonate with a specific radioactivity: 108.25 μCi/mg, 1.92 mCi/mmol. and in a radiochemical yield of 50% of the theoretical amount.