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An improved synthesis of ethanal‐1‐ 13 C
Author(s) -
Barbry Didier,
Couturier Daniel
Publication year - 1987
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/jlcr.2580240516
Subject(s) - chemistry , tributyltin hydride , palladium , sodium , medicinal chemistry , sodium hydride , chloride , chemical synthesis , stereochemistry , radiochemistry , organic chemistry , catalysis , biochemistry , in vitro
The title compound is obtained from sodium acétate‐1‐ 13 C by a shorter synthesis than the usual one. In the last step, acetyl chloride‐1‐ 13 C is reduced by tributyltin hydride with palladium (O) complexe.