Synthesis of U‐ 14 C‐labelled 5‐hydroxymethyl‐2‐furaldehyde | Zendy

Germond J. J. | Zendy; Arnaud M. M. | Zendy

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Synthesis of U‐ 14 C‐labelled 5‐hydroxymethyl‐2‐furaldehyde

Author(s) -

Germond J. J.,

Arnaud M. M.

Publication year - 1987

Publication title -

journal of labelled compounds and radiopharmaceuticals

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.432

H-Index - 47

eISSN - 1099-1344

pISSN - 0362-4803

DOI - 10.1002/jlcr.2580240316

Subject(s) - chemistry , hydroxymethyl , yield (engineering) , ketone , dehydration , fructose , ion exchange resin , high performance liquid chromatography , chromatography , nuclear chemistry , radiochemistry , organic chemistry , biochemistry , materials science , metallurgy

Uniformally 14 C‐labelled 5‐hydroxymethyl‐2‐furaldehyde was synthesized by dehydration of D‐[U‐ 14 C]fructose on an H + ion exchange resin and a water isobutylmethyl ketone biphasic liquid reaction medium. The optimal reaction time was 45min, and after HPLC purification the radiochemical yield was 50%. The whole process took 2 hours.

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