Syntheses of 1‐dodecyl‐d 25  phosphate | Zendy

Sniegoski Lorna T. | Zendy; White Edward | Zendy

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Syntheses of 1‐dodecyl‐d 25 phosphate

Author(s) -

Sniegoski Lorna T.,

White Edward

Publication year - 1983

Publication title -

journal of labelled compounds and radiopharmaceuticals

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.432

H-Index - 47

eISSN - 1099-1344

pISSN - 0362-4803

DOI - 10.1002/jlcr.2580200217

Subject(s) - chemistry , dodecanol , phosphate , deuterium , yield (engineering) , hydrogen phosphate , nuclear chemistry , catalysis , inorganic chemistry , medicinal chemistry , organic chemistry , physics , materials science , quantum mechanics , metallurgy

1‐Dodecyl‐d 25 phosphate was prepared from commercially available 1‐dodecanol‐d 26 . The 1‐dodecanol‐d 26 reacted with diphenyl phosphorochloridate to produce 1‐dodecyl‐d 25 diphenyl phosphate, which was reduced with hydrogen in the presence of Adams catalyst to give a 58.9 percent yield of 1‐dodecyl‐d 25 phosphate with 99.4 atom percent deuterium.

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