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Synthese d'Analogues Deuteries des (5α) Androstanediol ‐ 3ξ, 17β
Author(s) -
Jacolot F.,
Berthou F.,
Picart D.,
Le Gall J. Y.,
Floch H. H.
Publication year - 1982
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/jlcr.2580190410
Subject(s) - chemistry , deuterium , molecule , isotope dilution , mass spectrometry , dilution , analytical chemistry (journal) , radiochemistry , nuclear physics , organic chemistry , chromatography , thermodynamics , physics
Abstract Six deuterated androstanediols were synthetised. The position of deuterium atoms on the molecule were checked by mass spectrometry and 1 H or 13 c nuclear magnetic resonance. The per cent of d 0 , d 1 ,… d n ‐molecules were calculated. The use of such labelled molecules in the fields of isotopic dilution‐mass fragmentography as carriers and/or internal standards is discussed.