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9‐α‐D‐Arabinofuranosyl‐8‐azaadenine‐2‐ 14 C
Author(s) -
Montgomery John A.,
Thomas H. Jeanette
Publication year - 1978
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/jlcr.2580150187
Subject(s) - chemistry , nucleoside , acetic anhydride , carboxamide , chromatography , stereochemistry , organic chemistry , catalysis
Abstract 9‐α‐D‐Arabinofuranosyl‐8‐azaadenine‐2‐ 14 C ( 6 ) was prepared by a procedure previously described for the unlabeled nucleoside. The 14 C was incorporated into the 8‐azapurine by closure of 5‐amino‐v‐triazole‐4‐carboxamide with 14 C‐formic‐acetic anhydride. The labeled nucleoside ( 6 ) was purified by chromatography.