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Synthese des tritiummarkierten eberpheromons [5α, 6α‐ 3 H]‐5α‐androst‐16‐en‐3‐on
Author(s) -
Wagner H.,
Römer J.
Publication year - 1978
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/jlcr.2580140611
Subject(s) - chemistry , ketone , catalysis , specific activity , medicinal chemistry , radiochemistry , organic chemistry , enzyme
The synthesis of [5α, 6α‐ 3 H]‐5α‐androst‐16‐en‐3‐one, starting with the catalytic tritiation of 3β‐acetoxy‐androst‐5‐en‐17‐one, is described. The so‐called “boar taint ketone” was obtained with high specific activity (21 Ci/mmol) and radiochemical purity better than 98 %.