A simple and efficient synthesis of [ 2 H 10 ]deuterated bromfenvinphos by the Perkow reaction | Zendy

Huras Bogumiła | Zendy; Konopski Leszek | Zendy; Zakrzewski Jerzy | Zendy

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A simple and efficient synthesis of [ 2 H 10 ]deuterated bromfenvinphos by the Perkow reaction

Author(s) -

Huras Bogumiła,

Konopski Leszek,

Zakrzewski Jerzy

Publication year - 2011

Publication title -

journal of labelled compounds and radiopharmaceuticals

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.432

H-Index - 47

eISSN - 1099-1344

pISSN - 0362-4803

DOI - 10.1002/jlcr.1885

Subject(s) - chemistry , deuterium , bromide , ethanol , medicinal chemistry , phosphorus trichloride , radiochemistry , organic chemistry , nuclear chemistry , nuclear physics , physics

( E,Z )‐2‐bromo‐1‐(2,4‐dichlorophenyl)vinyl bis[ethyl‐ 2 H 5 ] phosphate ([ 2 H 10 ]bromfenvinphos), a regiospecifically deuterium‐labelled pesticide, was synthesized in two steps starting from [ 2 H 6 ]ethanol, phosphorus trichloride and 2,4‐dichlorophenacylidene bromide, and fully characterized. The deuterated biologically active bromfenvinphos is an important compound for the advancement of environmental degradation testing and some mass spectrometric studies. Copyright © 2011 John Wiley & Sons, Ltd.

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