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Synthesis of [ 15 N 3 ]melamine and [ 13 C 3 ]cyanuric acid
Author(s) -
Luo Yong,
Zhang Liya,
Yang Weicheng,
Liu Weixia,
Lu Weijing,
Li Meihua
Publication year - 2011
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/jlcr.1835
Subject(s) - cyanuric acid , chemistry , melamine , urea , organic chemistry , nuclear chemistry
This report presents an efficient syntheses of two labelled internal standards [ 15 N 3 ]melamine and [ 13 C 3 ]cyanuric acid with the common substrates [ 15 N]NH 4 Cl and [ 13 C]urea, respectively. Both standards with excellent isotopic and chemical purities were prepared in good yields and could be used as internal standards without further purification. Copyright © 2010 John Wiley & Sons, Ltd.