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Synthesis and purification of [1,2‐ 13 C 2 ]coniferin
Author(s) -
Beejmohun Vickram,
Grand Eric,
Lesur David,
Mesnard François,
Fliniaux MarcAndré,
Kovensky José
Publication year - 2006
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/jlcr.1068
Subject(s) - lignan , chemistry , ferulic acid , glucoside , chromatography , organic chemistry , medicine , alternative medicine , pathology
The double labelled lignan precursors [1,2‐ 13 C 2 ]coniferin and the glucoside of [1,2‐ 13 C 2 ]ferulic acid were prepared by classical synthetic methods. Pure double labelled lignan precursors could only be obtained after separation from their contaminating Z ‐isomers and dihydro by‐products by high‐performance liquid chromatography. Copyright © 2006 John Wiley & Sons, Ltd.