Synthesis and Crystal Structure of a Bis[6.3.3]propellane | Zendy

Jamrozik Janusz | Zendy; Żeslawski Wojeciech | Zendy; Grochowski Jacek | Zendy; Serda Pawel | Zendy; Dauter Zbigniew | Zendy

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Synthesis and Crystal Structure of a Bis[6.3.3]propellane

Author(s) -

Jamrozik Janusz,

Żeslawski Wojeciech,

Grochowski Jacek,

Serda Pawel,

Dauter Zbigniew

Publication year - 1996

Publication title -

liebigs annalen

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.825

H-Index - 155

eISSN - 1099-0690

pISSN - 0947-3440

DOI - 10.1002/jlac.199619960416

Subject(s) - propellane , chemistry , dihedral angle , derivative (finance) , crystal structure , tetrahydrofuran , molecule , crystallography , stereochemistry , bicyclic molecule , organic chemistry , hydrogen bond , solvent , financial economics , economics

The bis[6.3.3]propellane 6 derivative of 2,2′,6,6′‐tetramethylbiphenyl was, in the final stage, synthesized by dehydration, of octaalcohol 5 . X‐ray structure analysis revealed the highly symmetric shape of the molecule and disordered oxygen atoms in the tetrahydrofuran rings. The dihedral angle between LSQ phenyl planes is 62.6(1)°.

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