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Synthesis and spectroscopic characterization of 15 N‐labeled hexaaminobenzene derivatives
Author(s) -
Wolff J. Jens,
Limbach HansHeinrich
Publication year - 1991
Publication title -
liebigs annalen der chemie
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.825
H-Index - 155
eISSN - 1099-0690
pISSN - 0170-2041
DOI - 10.1002/jlac.1991199101121
Subject(s) - chemistry , characterization (materials science) , nuclear magnetic resonance spectroscopy , benzene , spectroscopy , organic chemistry , nanotechnology , materials science , physics , quantum mechanics
Efficient syntheses of [ 15 N 6 ]‐labeled hexaaminobenzene ( 6 ), hexakis(dimethylamino)benzene ( 7 ) and 2,2′,2″‐trimethylbenzotris(imidazol) ( 1 ) are described. The compounds are characterized by 15 N CPMAS NMR spectroscopy.