A simple preparation of ethyl 2,5‐dimethylfuran‐3‐carboxylate and 2,5‐dimethylfuran‐3,4‐dicarboxylic acid from diethyl 2,3‐diacetylsuccinate | Zendy

Wang GangQiang | Zendy; Guan Zhi | Zendy; Tang RongChang | Zendy; Ostojic Zeljko | Zendy; Jones T. Nicholas | Zendy; Wu TingTing | Zendy; He YanHong | Zendy

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A simple preparation of ethyl 2,5‐dimethylfuran‐3‐carboxylate and 2,5‐dimethylfuran‐3,4‐dicarboxylic acid from diethyl 2,3‐diacetylsuccinate

Author(s) -

Wang GangQiang,

Guan Zhi,

Tang RongChang,

Ostojic Zeljko,

Jones T. Nicholas,

Wu TingTing,

He YanHong

Publication year - 2009

Publication title -

journal of heterocyclic chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.321

H-Index - 59

eISSN - 1943-5193

pISSN - 0022-152X

DOI - 10.1002/jhet.92

Subject(s) - chemistry , dicarboxylic acid , carboxylate , aqueous solution , organic chemistry , solvent , organic solvent , engineering , chemical engineering

A simple preparation of ethyl 2,5‐dimethylfuran‐3‐carboxylate ( 3 ), 2,5‐dimethylfuran‐3,4‐dicarboxylic acid ( 4 ), and diethyl 2,5‐dimethylfuran‐3,4‐dicarboxylate ( 5 ) by treatment of diethyl 2,3‐diacetylsuccinate ( 2 ) with aqueous HCl is reported. The reaction is performed under organic solvent free conditions from a readily available cheap starting material. J. Heterocyclic Chem., (2009).

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