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Synthesis and spectral characterization of a novel series of methylcinnamate derivatives of 15‐crown‐5
Author(s) -
Gündüz Cihan,
Salan Ümit,
Bulut Mustafa
Publication year - 2009
Publication title -
journal of heterocyclic chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.321
H-Index - 59
eISSN - 1943-5193
pISSN - 0022-152X
DOI - 10.1002/jhet.90
Subject(s) - chemistry , crown ether , crown (dentistry) , elemental analysis , solvent , spectral analysis , organic chemistry , combinatorial chemistry , stereochemistry , spectroscopy , ion , medicine , physics , dentistry , quantum mechanics
A series of novel methylcinnamate derivatives of 15‐crown‐5 have been synthesized. The derivatives of methylcinnamate have been prepared by a synthesis from the corresponding chromenone‐crown ether with MeONa/MeOH or KOH, CH 3 I, and DMSO as solvent. Novel compounds were characterized by elemental analysis, IR, 1 H NMR, and MALDI‐TOF. J. Heterocyclic Chem., 46, 567 (2009).
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