An efficient synthesis of polyhydroacridine derivatives by the three‐component reaction of aldehydes, amines and dimedone in ionic liquid | Zendy

Shi DaQing | Zendy; Ni SaiNan | Zendy; Shi JingWen | Zendy; Dou GuoLan | Zendy; Li XiaoYue | Zendy; Wang XiangShan | Zendy

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An efficient synthesis of polyhydroacridine derivatives by the three‐component reaction of aldehydes, amines and dimedone in ionic liquid

Author(s) -

Shi DaQing,

Ni SaiNan,

Shi JingWen,

Dou GuoLan,

Li XiaoYue,

Wang XiangShan

Publication year - 2008

Publication title -

journal of heterocyclic chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.321

H-Index - 59

eISSN - 1943-5193

pISSN - 0022-152X

DOI - 10.1002/jhet.5570450303

Subject(s) - dimedone , chemistry , ionic liquid , bromide , elemental analysis , proton nmr , organic chemistry , carbon 13 nmr , medicinal chemistry , nmr spectra database , ionic bonding , catalysis , ion , spectral line , physics , astronomy

In this paper the preparation of 3,3,6,6‐tetramethyl‐9,10‐diaryl‐1,2,3,4,5,6,7,8,9,10‐decahydroacridine‐1,8‐dione derivatives from aldehydes, aromatic amines and 5,5‐dimethyl‐1,3‐cyclohexanedione in 1‐n‐butyl‐3‐methylimidazolium bromide ([bmim]Br) is described. The structures of these compounds were characterized by elemental analysis, IR and 1 H NMR spectra and further confirmed by single crystal X‐ray diffraction analysis.

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