A new synthesis of 1,2,3,5‐tetrahydroimidazo[2,3‐ b ]‐[1,3]benzodiazocines | Zendy

In Cho Hyun | Zendy; Lee Seung Won | Zendy; Lee KeeJung | Zendy

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A new synthesis of 1,2,3,5‐tetrahydroimidazo[2,3‐ b ]‐[1,3]benzodiazocines

Author(s) -

In Cho Hyun,

Lee Seung Won,

Lee KeeJung

Publication year - 2004

Publication title -

journal of heterocyclic chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.321

H-Index - 59

eISSN - 1943-5193

pISSN - 0022-152X

DOI - 10.1002/jhet.5570410525

Subject(s) - chemistry , methyl acrylate , intramolecular force , cycloaddition , dehydration , stereochemistry , medicinal chemistry , organic chemistry , catalysis , biochemistry , copolymer , polymer

A new synthesis of 6‐carbomethoxy‐1,2,3,5‐tetrahydroirnidazo[2,3‐ b ][1,3]benzodiazocines 13 by the intramolecular cycloaddition reaction of methyl 2‐(1‐aziridinylmethyl)‐3‐(2‐ureidophenyl)propenoates 10 under Appel's dehydration conditions is described. The latter were readily obtained from 2‐nitrobenzalde‐hyde with methyl acrylate through the Baylis‐Hillman reaction.

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