New one step synthesis of crown compounds containing a 1,3,4‐thiadiazole moiety | Zendy

Bentiss Fouad | Zendy; Lebrini Mounim | Zendy; Lagrenée Michel | Zendy

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New one step synthesis of crown compounds containing a 1,3,4‐thiadiazole moiety

Author(s) -

Bentiss Fouad,

Lebrini Mounim,

Lagrenée Michel

Publication year - 2004

Publication title -

journal of heterocyclic chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.321

H-Index - 59

eISSN - 1943-5193

pISSN - 0022-152X

DOI - 10.1002/jhet.5570410319

Subject(s) - chemistry , moiety , nucleophilic substitution , anhydrous , polymer chemistry , nucleophile , nuclear magnetic resonance spectroscopy , polyethylene glycol , base (topology) , ethylene glycol , potassium carbonate , organic chemistry , mathematical analysis , mathematics , catalysis

New macrocyclic polyether compounds containing a 2,5‐bis(2‐hydroxyphenyl)‐1,3,4‐thiadiazole moiety have been prepared by a nucleophilic substitution reaction involving ethylene or polyethylene glycol ditosylate and a bisphenol, the 2,5‐bis(2‐hydroxyphenyl)‐1,3,4‐thiadiazole, with solid anhydrous carbonate as a base. The structures of the macrocycles obtained were firmly established by 1 H and 13 C nmr spectroscopy and their mass spectra.

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