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Synthesis of methyl‐2,4‐bis(cyclohexane)dispiro‐1,2,3,4,4a,5,6,7‐octahydro‐(l H ,3 H )quinazoline‐8‐carbodithioate derived from cyclohexanone in one step
Author(s) -
Contreras Ricardo R.,
Fontal Bernardo,
Reyes Marisela,
Suárez Trino,
Bellandi Fernándo,
Bahsas All
Publication year - 2001
Publication title -
journal of heterocyclic chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.321
H-Index - 59
eISSN - 1943-5193
pISSN - 0022-152X
DOI - 10.1002/jhet.5570380532
Subject(s) - cyclohexanone , chemistry , cyclohexane , quinazoline , carbon disulfide , medicinal chemistry , disulfide bond , mass spectrum , spectroscopy , carbon 13 nmr , proton nmr , stereochemistry , organic chemistry , catalysis , ion , quantum mechanics , biochemistry , physics
The new compound Methyl‐2,4‐bis(cyclohexane)dispiro‐1,2,3,4,4a,5,6,7‐octahydro‐(1 H ,3 H )‐quinazo‐line‐8‐carbodithioate has been synthesized from cyclohexanone and carbon disulfide. It has been characterized by uv‐visible, FTTR , mass spectra and a complete structure proposed based on 1 H and 13 C NMR spectroscopy.