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Assignment of the Phosphorus, Proton and Carbon‐NMR Spectra of [(Tetrahydro‐2‐hydroxy‐5,5‐dimethyl‐4 H ‐1,4,2‐oxazaphosphorin‐4‐yl)methyl] phosphonic acid P ‐Oxide
Author(s) -
Dhawan Balram,
Redmore Derek,
Boyd Walter A.
Publication year - 1993
Publication title -
journal of heterocyclic chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.321
H-Index - 59
eISSN - 1943-5193
pISSN - 0022-152X
DOI - 10.1002/jhet.5570300638
Subject(s) - chemistry , methylene , phosphorus , medicinal chemistry , proton , phosphorus 31 nmr spectroscopy , carbon 13 nmr , proton nmr , nmr spectra database , carbon 13 , nuclear magnetic resonance spectroscopy , spectral line , stereochemistry , organic chemistry , physics , quantum mechanics , astronomy
The 1 H and 13 C nmr signals of the methylene groups directly linked to the phosphorus atoms, namely P(2)‐C(3)H 2 and P(8)‐C(7)H 2 in 1a were assigned with the help of hetronuclear decoupling experiments and HETCOR spectrum.