Identification of a 4 H ‐benz[ f ]indole by‐product from the friedel‐crafts‐based synthesis of benzoylpyrrole calcium channel activators | Zendy

Huber Edward W. | Zendy; Barbuch Robert J. | Zendy; Dalton Christopher R. | Zendy; Kane John M. | Zendy; Velayo Nelson L. | Zendy

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Identification of a 4 H ‐benz[ f ]indole by‐product from the friedel‐crafts‐based synthesis of benzoylpyrrole calcium channel activators

Author(s) -

Huber Edward W.,

Barbuch Robert J.,

Dalton Christopher R.,

Kane John M.,

Velayo Nelson L.

Publication year - 1993

Publication title -

journal of heterocyclic chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.321

H-Index - 59

eISSN - 1943-5193

pISSN - 0022-152X

DOI - 10.1002/jhet.5570300305

Subject(s) - chemistry , heteronuclear molecule , friedel–crafts reaction , indole test , calcium channel , stereochemistry , organic chemistry , calcium , combinatorial chemistry , nuclear magnetic resonance spectroscopy , catalysis

9,9a‐Dihydro‐2,9a‐dimethyl‐4‐oxo‐4 H ‐benz[ f ]indole‐3‐carboxylic acid, methyl ester was formed in varying amounts from the Friedel‐Crafts‐based synthesis of benzoylpyrrole calcium channel activators. The structure of this by‐product was determined using two‐dimensional long‐range 1 H‐ 13 C heteronuclear correlated and INADEQUATE nmr techniques.

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