A macrocyclic amide from dehydrochlorination of indole‐3‐carbonyl chloride | Zendy

Oliver J. E. | Zendy; Waters R. M. | Zendy; Lusby W. R. | Zendy; FlippenAnderson J. L. | Zendy

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A macrocyclic amide from dehydrochlorination of indole‐3‐carbonyl chloride

Author(s) -

Oliver J. E.,

Waters R. M.,

Lusby W. R.,

FlippenAnderson J. L.

Publication year - 1991

Publication title -

journal of heterocyclic chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.321

H-Index - 59

eISSN - 1943-5193

pISSN - 0022-152X

DOI - 10.1002/jhet.5570280619

Subject(s) - chemistry , tetramer , ketene , amide , indole test , ring (chemistry) , mass spectrometry , infrared spectroscopy , nuclear magnetic resonance spectroscopy , infrared , single crystal , crystal structure , stereochemistry , polymer chemistry , medicinal chemistry , crystallography , organic chemistry , physics , chromatography , optics , enzyme

Indolyl‐3‐ketene 3 was generated from two precursors and was found to form a symmetrical tetramer 4 consisting of a sixteen‐membered ring amide. The tetramer was characterized by mass spectrometry, infrared, 1 H and 13 C‐nmr spectroscopy, and single crystal X‐ray crystallography.

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