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Preparation of [2 3 ]cyclophane‐1,2‐diones by the reaction of 3,6;12,15‐Di‐1,4‐benzo[6.6](3,4)‐1,2,5‐thiadiazolocyclophanes with grignard reagents
Author(s) -
Hatta Taizo,
Mataka Shuntaro,
Tashiro Masashi
Publication year - 1986
Publication title -
journal of heterocyclic chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.321
H-Index - 59
eISSN - 1943-5193
pISSN - 0022-152X
DOI - 10.1002/jhet.5570230332
Subject(s) - cyclophane , chemistry , grignard reagent , grignard reaction , reagent , medicinal chemistry , stereochemistry , organic chemistry , crystal structure
3,6;12,15‐Di‐1,4‐benzo[6.6](3,4)‐1,2,5‐thiadiazolocyclophanes 1a‐c were prepared starting from 3,4‐di‐ p ‐tolyl‐1,2,5‐thiadiazole 3 and converted into [2 3 ]cyclophane‐1,2‐diones 2a‐c by the reaction with Grignard reagents.