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Synthesis and mass spectrum of 3‐(3′‐pyridinyloxymethyl)pyridine and polarography of its dialkyl diquaternary salts
Author(s) -
Attalla Moetaz I.,
Burnett Geoffrey R.,
Summers Lindsay A.
Publication year - 1985
Publication title -
journal of heterocyclic chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.321
H-Index - 59
eISSN - 1943-5193
pISSN - 0022-152X
DOI - 10.1002/jhet.5570220217
Subject(s) - chemistry , pyridine , polarography , alkyl , medicinal chemistry , mass spectrum , organic chemistry , inorganic chemistry , ion
3‐(3′‐Pyridinyloxymethyl)pyridine is prepared by reaction of 3‐hydroxymethylpyridine with 3‐bromopyridine and converted to the 1,1′‐dimethyl and 1,1′‐diethyl diquaternary salts with alkyl iodides. The salts are reduced polarographically at a potential (E o ) of about ‐ 1.02 to ‐ 1.10 V in the p H range of 5.5‐8.5.
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