Reactions of ethyl β‐methoxycrotonate with some  α,β ‐unsaturated carbonyl compounds. Synthesis of 6‐aroyl‐5‐aryl‐3‐methoxycyclohex‐2‐enones | Zendy

Shandala Mowafak Y. | Zendy; Ayoub Mikdad T. | Zendy; Kareem Ahmad A. | Zendy

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Reactions of ethyl β‐methoxycrotonate with some α,β ‐unsaturated carbonyl compounds. Synthesis of 6‐aroyl‐5‐aryl‐3‐methoxycyclohex‐2‐enones

Author(s) -

Shandala Mowafak Y.,

Ayoub Mikdad T.,

Kareem Ahmad A.

Publication year - 1984

Publication title -

journal of heterocyclic chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.321

H-Index - 59

eISSN - 1943-5193

pISSN - 0022-152X

DOI - 10.1002/jhet.5570210638

Subject(s) - chemistry , aryl , sodium hydride , hydride , medicinal chemistry , nuclear magnetic resonance spectroscopy , organic chemistry , metal , alkyl

3‐Aryl‐1‐phenyl‐2‐propen‐1‐ones Ia‐h and 1‐aryl‐3‐phenyl‐2‐propen‐1‐ones Ii‐ℓreacted with ethyl β‐methoxy‐crotonate (II) in the presence of sodium hydride in dry THF at 0° for 10 hours to give the corresponding 6‐aroyl‐5‐aryl‐3‐methoxy‐2‐cyclohexen‐1‐ones III. The structures of the products were confirmed by ir, pmr, 13 C nmr and uv spectroscopy.

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