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The assignment of the 1 H‐NMR and 13 C‐NMR spectra of 5 H ‐dibenz[ b,f ]azepine and 10,11‐dihydro‐5 H ‐dibenz[ b,f ]azepine
Author(s) -
Hallberg A.,
AlShowaier I.,
Martin A. R.
Publication year - 1984
Publication title -
journal of heterocyclic chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.321
H-Index - 59
eISSN - 1943-5193
pISSN - 0022-152X
DOI - 10.1002/jhet.5570210139
Subject(s) - azepine , chemistry , nmr spectra database , spectral line , carbon 13 nmr , carbon 13 nmr satellite , stereochemistry , nuclear magnetic resonance spectroscopy , proton nmr , medicinal chemistry , fluorine 19 nmr , physics , astronomy
The total assignments of the 1 H‐nmr and 13 C‐nmr spectra of 5 H ‐dibenz[ b,f ]azepine [1] and 10,11‐dihydro‐5 H ‐dibenz[ b,f ]azepine ( 2 ) have been made based on comparison with the corresponding 4,6‐dideuterated derivatives 3 , and 4 . These compounds were prepared via repeated lithiations and subsequent deuterations of 1 and 2 .