Identification of the nitrosation reaction products of alkyl esters of 1,2‐benzisoxazole‐3‐acetic acid by chemical and crystallographic methods | Zendy

Giannella Mario | Zendy; Gualtieri Fulvio | Zendy; Fedeli Walter | Zendy; Cerrini Silvio | Zendy; Gavuzzo Enrico | Zendy

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Identification of the nitrosation reaction products of alkyl esters of 1,2‐benzisoxazole‐3‐acetic acid by chemical and crystallographic methods

Author(s) -

Giannella Mario,

Gualtieri Fulvio,

Fedeli Walter,

Cerrini Silvio,

Gavuzzo Enrico

Publication year - 1983

Publication title -

journal of heterocyclic chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.321

H-Index - 59

eISSN - 1943-5193

pISSN - 0022-152X

DOI - 10.1002/jhet.5570200223

Subject(s) - chemistry , acetic acid , nitrosation , nitrite , alkyl , organic chemistry , carboxylic acid , crystal structure , amyl nitrite , medicinal chemistry , nitrate , medicine , anesthesia

The reaction between methyl or ethyl esters of 1, 2‐benzisoxazole‐3‐acetic acid and iso ‐amyl nitrite is reported. The main product is identified as 4‐(2′‐hydroxyphenyl)furazan‐3‐carboxylic acid ( 4 ) by chemical and X‐ray crystal structure analyses. The synthesis of esters of E ‐ and Z ‐α‐(hydroxyimino)‐1, 2‐benzisoxazole‐3‐acetic acid is also reported.

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