Synthesis in the diazasteroid group X . A synthesis of 8,12‐diaza‐ D ‐homosteroid | Zendy

Yamazaki Takao | Zendy; Takahata Hiroki | Zendy; Hama Yoko | Zendy; Takano Yoshiaki | Zendy; Nagata Masanori | Zendy; Castle Raymond N. | Zendy

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Synthesis in the diazasteroid group X . A synthesis of 8,12‐diaza‐ D ‐homosteroid

Author(s) -

Yamazaki Takao,

Takahata Hiroki,

Hama Yoko,

Takano Yoshiaki,

Nagata Masanori,

Castle Raymond N.

Publication year - 1979

Publication title -

journal of heterocyclic chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.321

H-Index - 59

eISSN - 1943-5193

pISSN - 0022-152X

DOI - 10.1002/jhet.5570160323

Subject(s) - chemistry , acetic anhydride , acetylation , condensation , tetrahydroisoquinoline , group (periodic table) , catalysis , medicinal chemistry , organic chemistry , stereochemistry , biochemistry , physics , thermodynamics , gene

The condensation of 1‐aminoethyl‐6,7‐dimethoxy‐1,2,3,4‐tetrahydroisoquinoline 1 with 1,2‐cyclohexanedione 2 gave the 8,12‐diaza‐ D ‐homosteroid system 3 , which was reduced with Adams' catalyst followed by acetic anhydride acetylation to afford the 8,12‐diaza‐ D ‐homosteroids 4a,b .

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