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Synthesis and spectroscopic properties of some di‐ and trideuterated methylpyridines
Author(s) -
Pavlik James W.,
Vongnakorn Tharinee,
Tantaya Supawan
Publication year - 2009
Publication title -
journal of heterocyclic chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.321
H-Index - 59
eISSN - 1943-5193
pISSN - 0022-152X
DOI - 10.1002/jhet.55
Subject(s) - chemistry , deuterium , nmr spectra database , stereochemistry , spectral line , medicinal chemistry , physics , quantum mechanics , astronomy
2‐Trideuteriopyridine‐4,6‐d 2 ( 1‐4,6‐d 2 ), 3‐methylpyridine‐2,6‐d 2 ( 2‐2,6‐d 2 ), 3‐methylpyridine‐2,4,6‐d 3 ( 2‐2,4,6‐d 3 ), and 4‐trideuteriopyridine‐2,6‐d 2 ( 3‐2,6‐d 2 ) were synthesized from the appropriate 2‐, 3‐, or 4‐methylpyridine N‐oxides. These deuterated products were characterized by their 1 H NMR and 13 C NMR spectra. J. Heterocyclic Chem., 46 , 213 (2009).