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Investigation of the Reaction of In Situ Prepared Dithiocarbamic Acids with Itaconic Anhydride in Water
Author(s) -
Halimehjani Azim Ziyaei,
Nosood Yazdanbakhsh Lotfi
Publication year - 2017
Publication title -
journal of heterocyclic chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.321
H-Index - 59
eISSN - 1943-5193
pISSN - 0022-152X
DOI - 10.1002/jhet.2957
Subject(s) - chemistry , carbon disulfide , succinic anhydride , acetic anhydride , primary (astronomy) , itaconic acid , organic chemistry , dithiocarbamate , alkyl , carbamate , acetic acid , catalysis , copolymer , polymer , physics , astronomy
An environmentally benign procedure for the synthesis of 2‐(3‐alkyl‐4‐oxo‐2‐thioxo‐1,3‐thiazinan‐5‐yl)acetic acid via the one‐pot three‐component reaction of primary amines, carbon disulfide, and itaconic anhydride in water is described. Also, this protocol was expanded for the synthesis of succinic acids containing a dithiocarbamate group by using hindered primary amines and secondary amines.

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