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Improved preparation of 3‐(1,1‐dimethylallyl)decursinol
Author(s) -
Jiang Xiangrui,
Li Jianfeng,
Zhang Rongxia,
Guo Hongli,
Huang Shaolei,
Shen Jingshan
Publication year - 2009
Publication title -
journal of heterocyclic chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.321
H-Index - 59
eISSN - 1943-5193
pISSN - 0022-152X
DOI - 10.1002/jhet.105
Subject(s) - chemistry , yield (engineering) , silica gel , catalysis , nuclear chemistry , chromatography , organic chemistry , metallurgy , materials science
An improved preparation method of 3‐(1,1‐dimethylallyl)decursinol from inexpensive commercially available start material was described. In the cyclization of 13 , silica gel was used as catalyst to give 1 with high purity and satisfying yield. J. Heterocyclic Chem., 46, 560 (2009).