Acid catalyzed pressure synthesis of  N,N ‐dimethylbenzylamine from benzylamine and methanol | Zendy

Nandi Dilip K. | Zendy; Palit Sunanda K. | Zendy; Deka Dibakar C. | Zendy

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Acid catalyzed pressure synthesis of N,N ‐dimethylbenzylamine from benzylamine and methanol

Author(s) -

Nandi Dilip K.,

Palit Sunanda K.,

Deka Dibakar C.

Publication year - 1987

Publication title -

journal of chemical technology and biotechnology

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.64

H-Index - 117

eISSN - 1097-4660

pISSN - 0268-2575

DOI - 10.1002/jctb.280380404

Subject(s) - benzylamine , hydrochloric acid , methanol , catalysis , chemistry , nuclear chemistry , organic chemistry

The synthesis of N,N ‐dimethylbenzylamine from benzylamine and methanol in the presence of hydrochloric acid catalyst has been carried out under pressure. Nitrogen pressure is helpful only to a limited extent, beyond which it is neither helpful nor detrimental. Under optimum conditions (517 K, 6.0295 MPa, residence period 2 h, benzylamine‐to‐methanol‐to‐hydrochloric acid mol ratio 1:2:1) the conversion of benzylamine to N,N ‐dimethylbenzylamine is 57.09%.

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