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Synthesis of Silver Nanoparticles Using Ionic‐Liquid‐Based Microwave‐Assisted Extraction from Polygonum minus and Photodegradation of Methylene Blue
Author(s) -
Ullah Habib,
Wilfred Cecilia Devi,
Shaharun Maizatul Shima
Publication year - 2017
Publication title -
journal of the chinese chemical society
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.329
H-Index - 45
eISSN - 2192-6549
pISSN - 0009-4536
DOI - 10.1002/jccs.201700144
Subject(s) - chemistry , ionic liquid , photodegradation , silver nanoparticle , fourier transform infrared spectroscopy , methylene blue , nuclear chemistry , dynamic light scattering , extraction (chemistry) , silver nitrate , spectrophotometry , nanoparticle , analytical chemistry (journal) , photocatalysis , chromatography , organic chemistry , nanotechnology , chemical engineering , catalysis , materials science , engineering
A green biogenic, nontoxic, high‐yielding synthetic method is introduced for the synthesis of silver nanoparticles (AgNPs) using ionic‐liquid‐based, microwave‐assisted extraction (ILMAE) from Polygonum minus . The aqueous ionic liquid (1‐butyl‐3‐methylimidazolium chloride [BMIM]Cl)‐based plant extract was used as reducing agent to reduce silver ions to AgNPs. The synthesis of AgNPs was confirmed by UV–visible spectrophotometry. Fourier transforms infrared (FTIR) spectra showed that the plant bioactive compounds capped the AgNPs. The particle size and morphology of Ag NPs were characterized by dynamic light scattering (DLS) and field emission scanning electron microscopy (FESEM), respectively. Elemental analysis was carried out by energy‐dispersive X‐ray (EDX) spectroscopy. Photodegradation studies showed that the AgNPs degraded 98% of methylene blue in 12 min.