Facile Solid‐Phase Organic Synthesis of 5‐Vinyl‐Substituted 1,2,4‐Oxadiazoles from Polymer‐Bound α‐Selenopropionic Acid | Zendy

Hu QiaoSheng | Zendy; Sheng ShouRi | Zendy; Liu XiaoLing | Zendy; Hu Fang | Zendy; Cai MingZhong | Zendy

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Facile Solid‐Phase Organic Synthesis of 5‐Vinyl‐Substituted 1,2,4‐Oxadiazoles from Polymer‐Bound α‐Selenopropionic Acid

Author(s) -

Hu QiaoSheng,

Sheng ShouRi,

Liu XiaoLing,

Hu Fang,

Cai MingZhong

Publication year - 2008

Publication title -

journal of the chinese chemical society

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.329

H-Index - 45

eISSN - 2192-6549

pISSN - 0009-4536

DOI - 10.1002/jccs.200800115

Subject(s) - chemistry , polystyrene , yield (engineering) , hydrochloride , polymer , phase (matter) , solid phase synthesis , organic chemistry , polymer chemistry , nuclear chemistry , peptide , biochemistry , materials science , metallurgy

Cyclocondensation of polystyrene‐supported α‐selenopropionic acid with amidoximes in the presence of 1‐(3‐dimethylaminopropyl)‐3‐ethylcarbodiimide hydrochloride (EDC) followed by oxidative deselenation efficiently afforded 5‐vinyl 1,2,4‐oxadiazoles in good yield and purity with a facile work‐up procedure.

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