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A Facile Preparation of Tebbe Reagent and its Subsequent Reactions
Author(s) -
Chou TaShue,
Huang SungBen,
Hsu WenHu
Publication year - 1983
Publication title -
journal of the chinese chemical society
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.329
H-Index - 45
eISSN - 2192-6549
pISSN - 0009-4536
DOI - 10.1002/jccs.198300044
Subject(s) - reagent , chemistry , solvent , organic chemistry , wittig reaction
A facile preparation of Tebbe reagent (1) by reacting AlMe 3 solution with Cp 1 TiCl 2 is reported. After complete removal of solvent and excess of AlMe 3 , the crude Tebbe reagent could be used without purification to react with ketones in a Wittig‐type manner.