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Catalyst‐Free One‐Pot Synthesis of Ketene Imines under Ultrasound Irradiation
Author(s) -
Emtiazi Hamideh,
Amrollahi Mohammad A.
Publication year - 2014
Publication title -
helvetica chimica acta
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.74
H-Index - 82
eISSN - 1522-2675
pISSN - 0018-019X
DOI - 10.1002/hlca.201400002
Subject(s) - chemistry , ketene , isocyanide , acetylenedicarboxylate , catalysis , combinatorial chemistry , organic chemistry
An efficient and simple procedure for the synthesis of ketene imines via a one‐pot three‐component reaction of cyclohexyl isocyanide, diethyl acetylenedicarboxylate, and 1,4‐dihydropyridines under ultrasonic irradiation is described. The remarkable advantages are the simplicity of the experimental procedures, high yields, and short reaction times.

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