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Synthesis and Spectroscopic Characterization of N 2 ‐( N ‐Acetyl‐6‐ O ‐stearoyl‐α‐ D ‐muramoyl)‐ L ‐alanyl‐ D ‐isoglutamine
Author(s) -
Dick Fritz,
Jenny Titus A.
Publication year - 1993
Publication title -
helvetica chimica acta
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.74
H-Index - 82
eISSN - 1522-2675
pISSN - 0018-019X
DOI - 10.1002/hlca.19930760819
Subject(s) - chemistry , characterization (materials science) , stereochemistry , nuclear magnetic resonance spectroscopy , combinatorial chemistry , nanotechnology , materials science
Title compound 1 was synthesized by a published route which had to be modified (seven steps from readily obtainable starting materials). Characterization of 1 was achieved by spectroscopic means (FAB‐MS, 1 H‐NMR, including 2D‐COSY). Furthermore, commercially available reference material purchased for comparison, was unequivocally established to be 10 , i.e. incompletely deprotected 1 .