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Reaction of Anthranilamide with Phosphorus Pentasulfide: Formation of 2‐Mercapto‐(1 H )‐1,3,2λ 5 ‐benzodiazaphosphorine‐2,4‐dithione
Author(s) -
Nagarajan Kuppuswamy,
Shenoy Sharada J.,
Fritz Hans,
Hosang Othmar,
Richter Wilhelm J.
Publication year - 1985
Publication title -
helvetica chimica acta
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.74
H-Index - 82
eISSN - 1522-2675
pISSN - 0018-019X
DOI - 10.1002/hlca.19850680411
Subject(s) - chemistry , pyridine , salt (chemistry) , boiling , elemental analysis , phosphorus , mass spectrum , organic chemistry , nuclear chemistry , medicinal chemistry , ion
The reaction of anthranilamide with phosphorus pentasulfide in boiling pyridine leads to the benzodiazaphosphorine‐pyridine salt 2 . The structure is established by elemental analysis, 1 H‐ 13 C‐ 15 N‐ 31 P‐NMR, and mass spectral data.