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Die Jodierung von desaktivierten aromatischen Aminen in wässeriger Phase
Author(s) -
Toth I.
Publication year - 1971
Publication title -
helvetica chimica acta
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.74
H-Index - 82
eISSN - 1522-2675
pISSN - 0018-019X
DOI - 10.1002/hlca.19710540533
Subject(s) - chemistry , aniline , yield (engineering) , iodine , hydrogen peroxide , medicinal chemistry , nitro , organic chemistry , alkyl , materials science , metallurgy
By treatment of deactivated aromatic amines such as 4‐nitroaniline, 4‐aminobenzonitrile or 2‐bromo‐4‐nitro‐aniline with iodine in water at 90–93° for 30–35 hours, in the presence of hydrogen peroxide, monoiodinated products with over 99% purity are obtained in 88–98% yield.
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