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Die Strukturen der mittleren Ringverbindungen. IX. 1, 8‐Diazacyclotetradecan‐dihydrobromid
Author(s) -
Dunitz J. D.,
Meyer E. F.
Publication year - 1965
Publication title -
helvetica chimica acta
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.74
H-Index - 82
eISSN - 1522-2675
pISSN - 0018-019X
DOI - 10.1002/hlca.19650480703
Subject(s) - chemistry , orthorhombic crystal system , crystallography , ring (chemistry) , group (periodic table) , crystal structure , stereochemistry , organic chemistry
Crystals of 1,8‐diazacyclotetradecane dihydrobromide are orthorhombic, a = 13.58, b = 14.81, c = 8.01 Å, Z = 4, space group Pccn (D 2h 10 ). The conformation of the 14‐membered ring has been established from three‐dimensional X‐ray analysis. It corresponds closely to an idealized conformation based on the diamond lattice.