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Analytical evaluation of laboratories wishing to perform environmental characterization studies
Author(s) -
Lauenstein Gunnar G.,
Cantillo Adriana Y.
Publication year - 1997
Publication title -
environmental toxicology and chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 1.1
H-Index - 171
eISSN - 1552-8618
pISSN - 0730-7268
DOI - 10.1002/etc.5620160702
Subject(s) - environmental science , contamination , trace (psycholinguistics) , mussel , environmental chemistry , analytical procedures , biochemical engineering , computer science , engineering , chemistry , ecology , biology , chromatography , philosophy , linguistics
Laboratories competing to analyze bivalve mollusks under contract to the National Oceanic and Atmospheric Administration's Mussel Watch Project were required to undergo analytical tests of their ability to quantify environmental contaminants as part of the contract evaluation process. During the 1989 selection process laboratories that appeared to qualify on the basis of their written proposals were provided a gravimetrically prepared solution with “unknown” quantities of an undefined number of organic contaminants that are regularly quantified for the Mussel Watch Project. In 1994, competing laboratories were once again tested but this time using matrix materials for the quantification of both trace elements and organic contaminants. Three laboratory groups participated in the exercises. For the 1989 gravimetrically prepared solutions, all participating laboratories were able to identify the contaminants present and in all but two cases were able to report values to within ±25% of the known values. In 1994, all laboratories were within the acceptance criteria for the quantification of trace elements in the homogenate sample. Analytical laboratory testing is an important first step to ensure that environmental characterization studies are successful.