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Electrochemical Characterization of Carbon Solidlike Paste Electrode Assembled Using Different Carbon Nanoparticles
Author(s) -
Malha Seif Islam Rabie,
Lahcen Abdellatif Ait,
Arduini Fabiana,
Ourari Ali,
Amine Aziz
Publication year - 2016
Publication title -
electroanalysis
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.574
H-Index - 128
eISSN - 1521-4109
pISSN - 1040-0397
DOI - 10.1002/elan.201500637
Subject(s) - carbon black , amperometry , materials science , dielectric spectroscopy , carbon fibers , electrode , electrochemistry , cyclic voltammetry , detection limit , graphite , chemical engineering , chemistry , composite number , chromatography , composite material , natural rubber , engineering
Solid like carbon paste electrodes (SCPEs) are built using different carbon materials namely carbon black N110, N220, N375, N772 and acetylene black. The electrochemical behavior of these electrodes and the influence of carbon black/paraffin ratio were studied and the results were discussed and compared to other electrodes prepared with graphite, mesoporous carbon and nanopowder carbon. Cyclic voltammetry, amperometry and electrochemical impedance spectroscopy were employed for their electrochemical and analytical characterizations. Amperometric measurements using N110, N220, N375 SCPEs with solid paraffin, showed a linear response of benzoquinone concentration with a detection limit of 75, 32 and 171 nM respectively.