Synthesis of Pyrene‐4,5‐dione on a 15 g Scale | Zendy

Walsh Joshua C. | Zendy; Williams KerryLynn M. | Zendy; Lungerich Dominik | Zendy; Bodwell Graham J. | Zendy

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Synthesis of Pyrene‐4,5‐dione on a 15 g Scale

Author(s) -

Walsh Joshua C.,

Williams KerryLynn M.,

Lungerich Dominik,

Bodwell Graham J.

Publication year - 2016

Publication title -

european journal of organic chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.825

H-Index - 155

eISSN - 1099-0690

pISSN - 1434-193X

DOI - 10.1002/ejoc.201601198

Subject(s) - chemistry , pyrene , yield (engineering) , combinatorial chemistry , scale (ratio) , scalability , product (mathematics) , organic chemistry , database , computer science , materials science , physics , geometry , mathematics , quantum mechanics , metallurgy

A scalable and efficient method for the synthesis of pyrene‐4,5‐dione has been developed. The addition of N ‐methylimidazole (NMI, 5 mol‐%) to a known oxidation reaction was shown to marginally improve the yield and dramatically improve the ease of the workup and thus the amount of product isolable in a day by using regular laboratory equipment.

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